PROCEDURE DETERMINATION OF PHOSPHORIC ACID IN THE SOFT DRINKS Black coloured soft drinks such as Coke from Coca Cola and Pepsi contains Phosphoric Acid in them. An experiment will be conducted here to determine the quantity of Phosphoric Acid content in the black coloured soft drinks. In the beginning of the experiment the preparation and standardization of a base solution will be made. Materials Required: 1. Pellets of Sodium Hydroxide (NaOH) 2. Phenolphthalein solution (1%) 3. Potassium acid phthalate (KHC8H4O4) 4. Graduated cylinder - 10 mL 5. Buffer solutions of pH 4 and 7 6. Graduated cylinder - 100 mL 7. Volumetric flask with stopper - 250 mL 8. Two 100-mL beakers 9. Two 50-mL Burettes 10. Two Small funnels so that they fit into …show more content…
The drop rate was adjusted to 1 to 2 drops/second. 10.0 mL of the NaOH solution was allowed to drip away into a waste beaker. The exact volume of the sodium hydroxide solution used was determined. A clean 250-mL beaker was taken and around 0.3 to 0.5 g of potassium acid phthalate was weighed into it. 50 mL of distilled water was approximately added to this 250 mL beaker and gently swirled so that the solid (potassium acid phthalate) got fully dissolved into the water. 2 drops of phenolphthalein indicator solution was added to the beaker. The pH electrode was calibrated using the pH buffers. For this, 25 mL of pH 4 and pH 7 buffers were taken in 50 mL or 100 mL beakers. The buffer solutions were saved in case the electrode needed to be re-calibrated later on. The potassium acid phthalate solution was titrated with 0.1 M NaOH. The solution turned red when it reached the end point. The titration was continued for 10 seconds after a permanent red color was obtained. The volume of 0.1 M NaOH solution used was determined. The 250 mL beaker was rinsed well with the distilled water. The titration procedure above was repeated 2 more times with fresh potassium acid
A hot plate was placed under the ring stand. 50 mL of 3.0 M NaOH in a 250 mL beaker and a stir bar was placed in the beaker. The beaker with NaOH was placed on the hot plate and 3.75 grams of NaAlO2*5H2O was placed in the beaker. The temperature probe was placed in the beaker with the solution, not touching the bottom of the beaker. The solution was heated and stirred till the solution dissolved.
Prelab week 1 Calculations Preparation of 1.5μmol/L mixed low-level standard dilution 150μmol/L × V1=1.5μmol/L × 10ml V1=(1.5μmol/L×10ml)/(150μmol/L)=0.1ml Conversion of milliliters to microliters (0.1ml×1000)μL= 100μL Preparation of 3μmol/L mixed low-level standard dilution 150μmol/L × V1=3μmol/L × 10ml V1=(3μmol/L×10ml)/(150μmol/L)=0.2ml Conversion of milliliters to microliters (0.2ml×1000)μL= 200μL Preparation of 3μmol/L mixed low-level standard dilution 150μmol/L × V1=7.5μmol/L × 10ml V1=(7.5μmol/L×10ml)/(150μmol/L)=0.5ml Conversion of milliliters to microliters (0.5ml×1000)μL= 500μL Preparation of the blank samples The volumetric flask will be filled to the mark with 150μmole/L of stock solution to act as blank (reference). Additional two blanks will
5. Question 5: a) As mentioned in the manual, we have the ratio (K/H+ ), if H+ was lower than K then the equivalent point will be achieved and it will change color. And if H+ was more than K then the solution we are titrating will be the same, the equivalent point won’t be achieved, and it will be acidic solution. And to find the value of H+ is by having the value of pH, therefore the pH has changed from 7 to 9, which is by shifting from 10-7 to 10 -8 by adding the 0.01 of the base, and it will shift again from 10 -8 to 10 -9 by adding another 0.01 of the base to the solution , the different that’s added between the two shifting are close to each other which indicates that the
Goals The primary goal of this experiment was to identify an unknown compound by running various tests to determine the qualitative solubility, conductivity, and pH value of the compound. Tests were also performed for the presence of specific cations and anions in the compound. The second goal was to discover the reactivity of the unknown compound by reacting it with different types of substances. The third goal of this project was to calculate the quantitative solubility of the unknown compound in water.
I. Purpose: To experimentally determine the mass and the mole content of a measured sample. II. Materials: The materials used in this experiment a 50-mL beaker, 12 samples, a balance and paper towels. III.
However, after refluxing for a while, yellow precipitates begin to form near the top of the flask. It was assumed that the remaining starting material was concentrated from a decrease volume to reappeared in solution. Nevertheless, this may have been a sign of contamination that will negatively affect the entire reaction. This observation later resulted in a yellowish
= 10^-3 M = 1,000 mL Here C1,C2; are the first and second concentrations of solution V1 and V2 ; are the required and current volumes. The impeller turned on and DDA, and tap water left to be mixed properly with water for 2 minutes. Approximately 150 grams of quartz added into the solution.
Weighed 1 gram of NaC2H3O2 and mixed it with ionized water. Boiled 12 mL of 1.0M Acetic Acid added into a beaker containing the sodium carbonate on a hot plate until all the liquid is evaporated
Standard Sodium hydroxide solution is the alkaline solution that will be used to titrate with soda water as it is a common solution that can be easily found in an ordinary school laboratory. It is a strong base. Carbonic acid is a weak acid which will react with a strong base to form a basic (pH > 7) solution. When Phenolphthalein is added to Soda water, the resultant solution is colourless. After titration with a strong base (sodium hydroxide), the solution will turn to pink as the solution becomes
A PH meter acts like a volt meter, and measures the water's amount of ”voltage”. Make sure the PH meter is calibrated before you use the probe to measure to potential hydrogen of the
Commercial vinegar, Yamaha brand 0.1 mol/dm3, NaOH soloution Phenolpthalein indicator soloution (50.00 ± 0.5 cm3 ) cm3 burrete (250.00 ± 0.5 cm3) volumetric flask a (250 cm3± 0.5 cm3)
Acids are proton donors in chemical reactions which increase the number of hydrogen ions in a solution while bases are proton acceptors in reactions which reduce the number of hydrogen ions in a solution. Therefore, an acidic solution has more hydrogen ions than a basic solution; and basic solution has more hydroxide ions than an acidic solution. Acid substances taste sour. They have a pH lower than 7 and turns blue litmus paper into red. Meanwhile, bases are slippery and taste bitter.
Practical I: Acid-base equilibrium & pH of solutions Aims/Objectives: 1. To determine the pH range where the indicator changes colour. 2. To identify the suitable indicators for different titrations. 3.
That caused a new initial reading of NaOH on the burette (see Table1 & 2). The drops were caused because the burette was not tightened enough at the bottom to avoid it from being hard to release the basic solution for titrating the acid. The volume of the acid used for each titration was 25ml. The volume of the solution was then calculated by subtracting the initial volume from the final volume. We then calculated the average volume at each temperature.
ABOUT THE SOFT DRINK INDUSTRY: The term "soft drink" refers to all types of nonalcoholic, carbonated, sweetened, flavored beverages. Nonalcoholic soft drink beverage market can be divided into fruit drinks and soft drinks. Soft drinks are available in glass bottles, aluminum cans; PET bottles are disposal containers can be divided into carbonated and non-carbonated drinks. Soft drinks are being manufactured since so long. There are various flavors in soft drinks that are lemon, orange, mango and cola.