Cyclohexene Lab Report

Cadet Eric Wiggins Date: 18 September 2014 Course Name: Chem 100 Instructor: Captain Zuniga Section: M3A Identification of a Copper Mineral Intro Minerals are elements or compounds that are created in the Earth by geological processes. The method of isolating metals in a compound mineral is normally conducted through two processes.

The lab started off by measuring critical materials for the lab: the mass of an an empty 100 mL beaker, mass of beaker and copper chloride together(52.30 g), and the mass of three iron nails(2.73 g). The goal of this experiment is to determine the number of moles of copper and iron that would be produced in the reaction of iron and copper(II) chloride, the ratio of moles of iron to moles of copper, and the percent yield of copper produced. 2.00 grams of copper(II) chloride was added in the beaker to mix with 15 mL of distilled water. Then, three dry nails are placed in the copper(II) chloride solution for approximately 25 minutes. The three nails have to be scraped clean by sandpaper to make the surface of the nail shiny; if the nails are not clean, then some unknown substances might accidentally mix into the reaction and cause variations of the result.

Stereoisomers Stereoisomers are isomeric molecules that have same molecular formula and sequence of bonded atoms, but differ in the arrangement of the atoms in space. The consideration of such spatial aspects of molecular structure is known as stereochemistry. Stereoisomers can be classified into two general categories: • Conformational isomers Isomers that differ in relative position of some of the atoms in the molecule in 3D-space due to the rotation about formally single bonds (sigma bonds). • Configurational isomers Isomers that arise due to some kind of rigidity in the molecule and they can be interconverted only by bond breaking or making.

The dehydration of 2-methylcyclohexanol takes place at the bottom of the Hickman still. As the Hickman still heats up within the sand bath, the products evaporate and travel higher up in the still where they condense into a liquid and fall within the collection ring, thus separating the product from the remaining water. Drierite (CaSO4) is also added as a drying agent to absorb any leftover water within the product. The purity of the product will then be analyzed with infrared spectroscopy, paying attention to OH peak if it is present. Chemical Reactions: Data and Observations: Material Volume Mol.

The ester studied was “3,” the acid used was 9.5 mL of “B,” and the alcohol used was 18.1 mL of “C.” A few substances were added to augment the production of the ester. Sulfuric acid (H2SO4) was added using a dropper bottle to catalyze the reaction. The desiccant in this reaction was drierite and was used to absorb the water byproduct. This prevented the ester from breaking apart into its constituents. The cold finger condenser was used to trap evaporated gas from the heated mixture, and condense it back into

The following lab period the solid was weighed (0.0483 g) and percent yield was calculated (65.5%) with the limiting reagent being tetraphenylcyclopentadienone. The melting point was determined. The first melting point was 204-204.9 °C and the second melting point was 215.6-215.9°C. Finally, an infrared spectroscopy was obtained for the

Referring to Table 1, the reactants for each run were transferred to an Erlenmeyer Flask (250 mL) via a buret. Using a precision pipette, the volume of I3- required for each run was carefully extracted and poured into the flask containing all of the reactants. Immediately after the Iodine solution was placed in the flask, the LabQuest began collection data. Meanwhile, a small portion of the solution, was used to rinse the cuvette, then using a disposable pipette a small amount of the solution was transferred to the cuvette (approx. ¾).

Murder and a Meal: An Organic Compounds Lab Problem: Based on the contents of the victim's stomach, where did he eat his final meal? Background Information: A macromolecule is a molecule that contains a large number of atoms, such as proteins, nucleic acids, carbohydrates or lipids. Macromolecules are formed by a process known as polymerization in which large compounds are built by the joining of smaller one together. The smaller units are known as monomers and monomers together form polymers. Macromolecules are important to living things for example

Experiment 5: Binary Liquid-Vapour Phase Diagram Student no.: 15226360 Date: 18-3-2016 Student name: Tong William Session: 3 Group: 7 Objective: To determine the conductivity of sodium chloride with different concentrations. To study the effect of concentration of acetic acid to the conductivity. To understand Onsager’s Equation Principle: The heterogeneous equilibrium between two phases in a system of two components is concerned in this experiment. The acetone-chloroform at 1 atm pressure system is studied.

TLC was used to identify the actual unknown product as well as other products/reactants present in the filtered solution. The procedure was conducted by placing a TLC plate in a developing chamber that is filled with a small amount of solvent. The solvent cannot be too polar because it will cause spotted compounds on the TLC plate to rise up too fast, while a very non-polar solvent will not allow the spots to move. The polarity of the spots also determines how far it moves on the plate; non-polar spots are higher than polar ones. After spots on the TLC form, the Rf values are calculated and used to analyze the similarity of the compounds.

Hydrogen chloride has a very powerful smell. It is in the form of a gas but only when it is at room temperature which is approximately 25 Celsius and when the pressure is high. When you add water to hydrogen chloride then it breaks down into small pieces which are known as dissolving. The solubility of hydrogen chloride is very high this means that it can dissolve in water quickly because it dissolves many times in its own solution (the gas form of hydrogen chloride). It is very soluble because the smaller the chain of the molecules are then the energy will be required in small quantities however if the chain is long then it will need more energy

There are two methods of obtaining cyclohexane. These two methods are fractional distillation of naphtha and hydrogenation of benzene. Research suggest that the hydrogenation of benzene is the most economical way to create our chemical of choice. According to ICIS, cyclohexane is used in the production of adipic acid used to

This was proved by utilizing the IR spectrum to verify the C =O was not in the final product as it lacked the 1640 cm-1 peak. The melting point of 113-115 degrees C proved that the final product obtained was the E-Stilbene. The TLC plate proved that the E and the Z product was produced, show cased by the double intensity of the DCM spot to the final product’s spot, both which had an Rf of 0.92. The double intensity proved that both products were produced, but through heating and filtering, the Z-Stilbene was

iv. 1,4 cyclohexanedimethanol (1,4 CHDM) 1,4 cyclohexanedimethanol is an alicyclic glycol [52], the cycloaliphatic structure of 1,4 cyclohexanedimethanol imparts particular conformational transitions and molecular structure to polyesters [53]. Ni et al [54] stated that polyesters containing cyclic moieties in their backbone are of transitional mechanical properties in comparison to aromatic and linear polyesters. 1,4 cyclohexanedimethanol could provide an excellent compromise between hardness and flexibility.

Introduction Cyclodextrins (CDs) are cyclic oligosaccharides consist of (α-1,4)-linked α-D-glucopyranose units produced by bacterial digestion of cellulose. These structurally related natural products contain a central cavity that was lined by the skeletal carbons and ethereal oxygens of the glucose residues, which gave it a lipophilic character to a certain extent while the outer surface is hydrophilic. The 3D-structure of CDs are shaped like a truncated cone rather than perfect cylinders due to the chair conformation of their glucopyranose units. The hydroxyl functional groups are orientated on the cone exterior with the primary hydroxyl groups of the sugar residues at the narrow edge of the cone, and the secondary hydroxyl groups at the wider edge. The polarity of the cavity has been estimated to be similar to that of an aqueous